oo Jumlada Shiinaha 2-Amino-5-chlorobenzophenone Soo saaraha Soo saaraha iyo Iibiyaha |LonGoChem
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Shiinaha 2-Amino-5-chlorobenzophenone Soo saaraha soo saaraha Sawirka
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2-Amino-5-chlorobenzophenone

Sharaxaad Gaaban:

Magaca alaabta: 2-Amino-5-chlorobenzophenone
CAS No.: 719-59-5
EINECS lambarka gelitaanka: 211-949-7
Qaaciddada molecular: C13H10ClNO
Miisaanka molecular: 231.68

Faahfaahinta Alaabta

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Qaab-dhismeedka

5
Jireed

Muuqaalka: Budada crystalline jaalaha ah
Cufnaanta: 1.33
Meesha dhalaalka: 96-98 °C (iftiin)
Barta karkarinta: 207 °C
Dib-u-celinta: 1.6000 (qiyaas)
Barta iftiimaya: 211 °C

Xogta Badbaadada
Guud ahaan

Codsiga
Metabolite-ka Diazepam;waxay lahayd saamayn anticonvulsant aad u daciif ah.

Dhexdhexaadiyeyaasha dawooyinka.Soo-saarka dawooyinka sida Librium iyo Valium.
Saamaynta deegaanka
In yar oo khatar ku ah biyaha, ha u oggolaan in tiro aan la qasin ama tiro badan ay la kulmaan biyaha dhulka hoostiisa ku jira, marin-biyoodyada ama hababka bulaacadaha, hana ku shubin walxaha deegaanka ku xeeran iyada oo aan oggolaansho laga helin dawladda.

Guryaha iyo Xasiloonida
Ku xasil heerkulka deegaanka iyo cadaadiska, iska ilaali taabashada oksaydhyada

Hababka kaydinta
Weelka si adag u xidh oo ku kaydi meel qabow oo qalalan weel si adag loo soo buuxiyay.

Habka synthesis
(1) Waxaa soo saaray falcelinta p-chloroaniline oo leh chloride benzoyl.Ku dar p-chlorobenzene dheriga falcelinta dhalada leh ee 70 ° C ama ka hooseeya, ku rid zinc chloride anhydrous, ku dar benzoyl chloride dropwise oo walaaqaya, ka dibna kor u qaad heerkulka, hay 195-205 ° C ilaa 2h, shan jeer ku dhaq biyaha kulul oo ah 90-95 ° C (lakabka biyaha iyo xalalka dhaqida ayaa soo kabanaya benzoic acid iyo zinc chloride) qiyaastii 100 ° C, ku dar sulfuric acid si tartiib ah, ku hay 142 ° C 40min.Cuncunku wuxuu ku da'ay biyo.Marka la walaaqayo, pH waxaa lagu hagaajiyaa alkali dareere ah oo aan ka sarreyn 1 waxaana lagu sifeeyaa 20-25 ° C.Sifeynta waxaa dib loogu soo celiyay p-chloroaniline.Keega shaandhada ayaa lagu qasaa oo lagu hakiyaa biyaha, la dhex dhexaadiyaa ilaa pH=6, la sifeeyay engegan, lagu dhaqa biyo dhexdhexaad ah oo la engejiyey si loo helo badeecada cayriin.Ka dib ku dar 6-7 jeer ethanol, 6% kaarboon firfircoon, reflux 30min, shaandheyn iyo crystallize, engegan si aad u hesho badeecada fiican.(2) p-Nitrochlorobenzene iyo cyanobenzyl giraanta isku darka si loo helo isoxazole, ka dibna fur giraanta, dhimista si aad u hesho.

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